6O6K
HUaa 19bp SYM DNA pH 5.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-05 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.115830 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 84.790, 84.790, 63.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.956 - 3.601 |
R-factor | 0.2571 |
Rwork | 0.252 |
R-free | 0.30190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4YEX and DNA |
RMSD bond length | 0.003 |
RMSD bond angle | 0.525 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.789 | 3.730 |
High resolution limit [Å] | 2.994 | 3.602 |
Rmerge | 0.135 | |
Rmeas | 0.141 | |
Number of reflections | 2939 | 18426 |
<I/σ(I)> | 15.1 | |
Completeness [%] | 99.7 | 98.6 |
Redundancy | 13.8 | 12.9 |
CC(1/2) | 1.000 | 0.245 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.02M ZnCl2, 20% PEG 3350 |