6O2F

GCN4 with NPEG4 at position 18

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR591
Temperature [K]	293
Detector technology	CCD
Collection date	2018-03-29
Detector	APEX II CCD
Wavelength(s)	1.55
Spacegroup name	I 21 21 21
Unit cell lengths	19.249, 30.046, 106.834
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.924 - 1.800
R-factor	0.1858
Rwork	0.180
R-free	0.23510
Data reduction software	PROTEUM PLUS
Data scaling software	PROTEUM PLUS
Phasing software	PHENIX
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall
Low resolution limit [Å]	28.924
High resolution limit [Å]	1.800
Number of reflections	3133
<I/σ(I)>	11.9
Completeness [%]	99.7
Redundancy	9.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	Pact Premier B1