6O2E

GCN4 with asparagine at position 18

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR591
Temperature [K]	293
Detector technology	CCD
Collection date	2018-03-29
Detector	APEX II CCD
Wavelength(s)	1.5406
Spacegroup name	I 21 21 21
Unit cell lengths	19.251, 30.016, 107.053
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	53.526 - 1.896
R-factor	0.2179
Rwork	0.214
R-free	0.24740
Data reduction software	PROTEUM PLUS
Data scaling software	PROTEUM PLUS
Phasing software	PHENIX
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall
Low resolution limit [Å]	53.526
High resolution limit [Å]	1.896
Number of reflections	4721

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	Pact premier C1