6O28
Crystal structure of 4493 Fab in complex with circumsporozoite protein KQPA and anti-kappa VHH domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-14 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.033200 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.958, 94.676, 143.989 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.237 - 1.930 |
R-factor | 0.1887 |
Rwork | 0.188 |
R-free | 0.21850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | In-house model |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.960 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.187 | 0.817 |
Rpim | 0.054 | 0.239 |
Number of reflections | 79786 | 3549 |
<I/σ(I)> | 9.4 | 1.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 13 | 12.8 |
CC(1/2) | 0.997 | 0.650 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M HEPES pH 7.0, 1 M lithium chloride, 20 % (w/v) PEG6000 |