6O16
Crystal structure of murine DHX37 in complex with RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-26 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0077 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.829, 137.593, 94.225 |
Unit cell angles | 90.00, 93.34, 90.00 |
Refinement procedure
Resolution | 47.032 - 2.875 |
R-factor | 0.2715 |
Rwork | 0.270 |
R-free | 0.29480 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.792 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.032 | 2.980 |
High resolution limit [Å] | 2.875 | 2.888 |
Rmerge | 0.103 | 0.625 |
Rmeas | 0.122 | 0.750 |
Rpim | 0.065 | 0.411 |
Number of reflections | 93431 | 4209 |
<I/σ(I)> | 9.76 | 1.57 |
Completeness [%] | 97.9 | 86.19 |
Redundancy | 3.4 | 3.1 |
CC(1/2) | 0.994 | 0.872 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.1 M Bis-Tris propane pH 7.0, 0.2 M NaNO3, 15% (w/v) polyethylene glycol (PEG) |