6O09
Structure of AtPCNA in complex with the PIP motif of ATXR6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-08-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 72.902, 90.549, 90.510 |
Unit cell angles | 60.05, 73.46, 73.59 |
Refinement procedure
Resolution | 29.652 - 2.060 |
R-factor | 0.1972 |
Rwork | 0.197 |
R-free | 0.23430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zvv |
RMSD bond length | 0.008 |
RMSD bond angle | 0.933 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.652 | 2.130 |
High resolution limit [Å] | 2.060 | 2.060 |
Number of reflections | 219871 | 10607 |
<I/σ(I)> | 9.2 | |
Completeness [%] | 94.4 | |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294.15 | 0.2 M sodium malonate 20% PEG3350 |