6NZ5
YcjX-GDPCP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.471, 128.257, 148.056 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.363 - 2.233 |
R-factor | 0.1798 |
Rwork | 0.178 |
R-free | 0.21700 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.577 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.260 |
High resolution limit [Å] | 2.220 | 2.220 |
Number of reflections | 54859 | |
<I/σ(I)> | 19 | |
Completeness [%] | 98.6 | |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 287 | 100 mM HEPES pH 6.5 and 6% (w/v) polyvinyl pyrrolidone |