6NVQ
Crystal structure of the VASH1-SVBP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-30 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.966 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.453, 128.929, 45.222 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.610 - 2.100 |
R-factor | 0.19839 |
Rwork | 0.198 |
R-free | 0.21428 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 1.220 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.610 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.062 | 1.538 |
Number of reflections | 24696 | 3536 |
<I/σ(I)> | 12.8 | 1.1 |
Completeness [%] | 99.7 | 51.8 |
Redundancy | 4.9 | 4.9 |
CC(1/2) | 0.990 | 0.518 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.8 | 293 | 19% PEG 3000, 0.1M Tris-HCl, 0.2M calcium chloride |