6NQF
Xanthomonas citri PGM Apo-Phospho at room temperature
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 298 |
Detector technology | CMOS |
Collection date | 2017-12-15 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.460, 55.490, 174.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.087 - 1.900 |
R-factor | 0.1712 |
Rwork | 0.170 |
R-free | 0.20530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.007 |
RMSD bond angle | 0.851 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.460 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.104 | 1.259 |
Rmeas | 0.118 | 1.442 |
Rpim | 0.054 | 0.685 |
Number of reflections | 34991 | 2215 |
<I/σ(I)> | 8.2 | 0.9 |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 4.7 | 4.3 |
CC(1/2) | 0.997 | 0.368 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |