6NQE
Xanthomonas citri PGM Apo-Dephospho at room temperature
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 298 |
Detector technology | CMOS |
Collection date | 2017-12-15 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.360, 55.620, 174.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.003 - 1.850 |
R-factor | 0.1621 |
Rwork | 0.161 |
R-free | 0.18730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.876 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.003 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.124 | 2.081 |
Rmeas | 0.134 | 2.254 |
Rpim | 0.051 | 0.852 |
Number of reflections | 37952 | 2257 |
<I/σ(I)> | 10.1 | 0.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.9 | 6.9 |
CC(1/2) | 0.997 | 0.375 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |