6NP8
Xanthomonas citri Phospho-PGM in complex with mannose-6-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2018-01-31 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.930, 54.300, 171.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.848 - 1.410 |
R-factor | 0.1811 |
Rwork | 0.179 |
R-free | 0.21310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.898 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.850 | 1.430 |
High resolution limit [Å] | 1.410 | 1.410 |
Rmerge | 0.084 | 1.715 |
Rmeas | 0.088 | 1.891 |
Rpim | 0.025 | 0.774 |
Number of reflections | 79996 | 2198 |
<I/σ(I)> | 21.1 | 0.8 |
Completeness [%] | 91.0 | 57.7 |
Redundancy | 12.2 | 5.7 |
CC(1/2) | 0.999 | 0.426 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |