6NOY
Structure of Cyanothece McdB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-12-19 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 95.500, 95.500, 177.100 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 74.937 - 3.460 |
| R-factor | 0.2301 |
| Rwork | 0.226 |
| R-free | 0.27160 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.745 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AutoSol |
| Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.000 | 3.650 |
| High resolution limit [Å] | 3.460 | 3.460 |
| Rpim | 0.047 | 0.653 |
| Number of reflections | 23328 | |
| <I/σ(I)> | 16.5 | 1.9 |
| Completeness [%] | 99.1 | 98.6 |
| Redundancy | 8.5 | 8.8 |
| CC(1/2) | 0.999 | 0.776 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 1.5 M ammonium sulfate, 0.1 M sodium acetate |
