6NNU
Xanthomonas citri Phospho-PGM in complex with glucose-1,6-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2018-03-28 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.690, 54.720, 173.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.296 - 1.460 |
R-factor | 0.1711 |
Rwork | 0.169 |
R-free | 0.20710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.005 |
RMSD bond angle | 0.848 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.300 | 1.480 |
High resolution limit [Å] | 1.460 | 1.460 |
Rmerge | 0.145 | 2.150 |
Rmeas | 0.151 | 2.286 |
Rpim | 0.041 | 0.759 |
Number of reflections | 73467 | 3579 |
<I/σ(I)> | 14.4 | 0.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.3 | 8.8 |
CC(1/2) | 0.999 | 0.345 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |