6NNT
Xanthomonas citri Dephospho-PGM in complex with glucose-1,6-bisphosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2017-12-15 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.620, 54.740, 173.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.198 - 1.450 |
R-factor | 0.1709 |
Rwork | 0.169 |
R-free | 0.20780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.908 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.200 | 1.470 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.114 | 2.421 |
Rmeas | 0.118 | 2.559 |
Rpim | 0.030 | 0.807 |
Number of reflections | 74685 | 3597 |
<I/σ(I)> | 17.1 | 0.9 |
Completeness [%] | 100.0 | 99.3 |
Redundancy | 14.9 | 9.8 |
CC(1/2) | 0.999 | 0.429 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 292 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |