6NNS
Xanthomonas citri Phospho-PGM in complex with glucose-6-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2018-03-28 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.720, 54.520, 172.480 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.561 - 1.450 |
R-factor | 0.1799 |
Rwork | 0.178 |
R-free | 0.21040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.844 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.080 | 1.470 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.117 | 1.724 |
Rmeas | 0.122 | 1.912 |
Rpim | 0.035 | 0.802 |
Number of reflections | 73075 | 3033 |
<I/σ(I)> | 16.4 | 0.7 |
Completeness [%] | 98.4 | 84.2 |
Redundancy | 11.9 | 5.4 |
CC(1/2) | 0.999 | 0.367 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |