6NNQ
Non-covalent structure of SENP1 in complex with SUMO2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 293.15 |
Detector technology | CCD |
Collection date | 2016-01-31 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 98.732, 98.732, 101.805 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.354 - 2.621 |
R-factor | 0.2313 |
Rwork | 0.229 |
R-free | 0.27660 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.532 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.240 | 2.740 |
High resolution limit [Å] | 2.620 | 2.620 |
Number of reflections | 15667 | |
<I/σ(I)> | 1.7 | |
Completeness [%] | 100.0 | |
Redundancy | 9.7 | |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 20% PEG 6000, 0.1M HEPES, pH 7.5 |