6NNO
Xanthomonas citri Phospho-PGM in complex with glucose-1-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2018-04-29 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.820, 54.570, 172.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.132 - 1.570 |
R-factor | 0.1717 |
Rwork | 0.170 |
R-free | 0.20620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.859 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.132 | 1.600 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.144 | 2.356 |
Rmeas | 0.150 | 2.506 |
Rpim | 0.041 | 0.839 |
Number of reflections | 58987 | 2988 |
<I/σ(I)> | 14.7 | 0.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 | 8.7 |
CC(1/2) | 0.999 | 0.332 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |