6NN1
Xanthomonas citri PGM Apo-Dephospho
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2017-12-15 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.020, 54.610, 171.960 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.020 - 1.500 |
R-factor | 0.1739 |
Rwork | 0.172 |
R-free | 0.20540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5bmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.840 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.020 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.107 | 2.950 |
Rmeas | 0.111 | 3.081 |
Rpim | 0.030 | 0.884 |
Number of reflections | 67541 | 3302 |
<I/σ(I)> | 14.8 | 0.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.3 | 12 |
CC(1/2) | 0.999 | 0.360 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 292 | 22% PEG 8000, 0.2M MgCl, 0.1M HEPES |