6NES
FAD-dependent monooxygenase TropB from T. stipitatus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-09 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.033 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 70.805, 184.494, 164.129 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.430 - 1.750 |
R-factor | 0.17 |
Rwork | 0.170 |
R-free | 0.19530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5evy |
RMSD bond length | 0.010 |
RMSD bond angle | 1.081 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.430 | 1.813 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.095 | 1.952 |
Rmeas | 0.098 | |
Rpim | 0.027 | |
Number of reflections | 107978 | |
<I/σ(I)> | 1.11 | |
Completeness [%] | 99.7 | |
Redundancy | 12.8 | |
CC(1/2) | 0.998 | 0.602 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 293.15 | 1.11 M ammonium tartrate dibasic, 6% hexanediol |