6NCQ
The dimerization domain of human SFPQ in space group C2221
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-04-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 65.131, 119.167, 72.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.490 - 1.900 |
R-factor | 0.204 |
Rwork | 0.201 |
R-free | 0.24300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wii |
RMSD bond length | 0.010 |
RMSD bond angle | 0.980 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.490 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 22646 | 1436 |
<I/σ(I)> | 15.8 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 4 | 4.1 |
CC(1/2) | 0.999 | 0.827 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl (pH 8,5), 35-40% (v/v) MPD |