6NBJ
Qri7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-01-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 180.315, 180.315, 180.315 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.060 - 2.940 |
R-factor | 0.20009 |
Rwork | 0.196 |
R-free | 0.26996 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.607 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.100 | 3.070 |
High resolution limit [Å] | 2.940 | 2.940 |
Number of reflections | 22014 | |
<I/σ(I)> | 8 | |
Completeness [%] | 99.8 | |
Redundancy | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 25% PEG 400, 3% w/v dextran sulfate sodium salt (Mr 5000), 0.1M HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |