6NA3
Crystal Structure of Apo-form of ECR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-29 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.980 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.100, 153.000, 202.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.966 - 1.800 |
R-factor | 0.1994 |
Rwork | 0.199 |
R-free | 0.24200 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.167 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.966 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 223907 | |
<I/σ(I)> | 12.32 | |
Completeness [%] | 91.5 | |
Redundancy | 6.14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 293 | 0.1M TRIS ph 8.0 20% w/v Poly(acrylic acid sodium salt) 5100 30% Glycerol |