6N9L
Crystal structure of T. maritima UvrA d117-399 with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 98.2 |
Detector technology | PIXEL |
Collection date | 2016-03-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 143.134, 81.379, 90.416 |
Unit cell angles | 90.00, 125.30, 90.00 |
Refinement procedure
Resolution | 38.049 - 2.010 |
R-factor | 0.1701 |
Rwork | 0.169 |
R-free | 0.20130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ux8 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.076 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.049 | 2.082 |
High resolution limit [Å] | 2.010 | 2.010 |
Number of reflections | 51809 | 4575 |
<I/σ(I)> | 8.42 | 1.09 |
Completeness [%] | 91.8 | 81.93 |
Redundancy | 3.9 | 3.5 |
CC(1/2) | 0.994 | 0.525 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 100 mM HEPES-NaOH, pH 7.5 and 22w/v PEG 3350 | |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 100 mM HEPES-NaOH, pH 7.5 and 22w/v PEG 3350 |