6N9B
FtsY-NG ultra high-resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-04-26 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.683, 76.180, 108.786 |
Unit cell angles | 90.00, 93.87, 90.00 |
Refinement procedure
Resolution | 44.200 - 1.219 |
R-factor | 0.1565 |
Rwork | 0.155 |
R-free | 0.17880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6cqp |
RMSD bond length | 0.012 |
RMSD bond angle | 1.114 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.200 | 1.263 |
High resolution limit [Å] | 1.219 | 1.219 |
Rmerge | 0.029 | |
Number of reflections | 165619 | |
<I/σ(I)> | 14.75 | |
Completeness [%] | 98.7 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 297.15 | 0.1 M Bis-Tris pH 6.6, 24% PEG 2000 MME, 200 mM KBr. |