6N8C
Structure of the Huntingtin tetramer/dimer mixture determined by paramagnetic NMR
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 600 | |
| 2 | Bruker | AVANCE III | 800 | |
| 3 | Bruker | AVANCE III | 900 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 2 | 2D 1H-15N HSQC |
| 10 | 2 | 4 | 1HN PRE |
| 11 | 1 | 6 | 13CA SQ CPMG |
| 12 | 1 | 6 | 15N SQ CPMG |
| 2 | 1 | 2 | 2D 1H-13C CT HSQC |
| 3 | 2 | 2 | 3D CBCA(CO)NH |
| 4 | 2 | 2 | 3D HNCACB |
| 5 | 2 | 4 | 3D TOCSY-HSQC |
| 6 | 1 | 3 | 13CA SQ CPMG |
| 7 | 1 | 5 | 13CA SQ CPMG |
| 8 | 1 | 3 | 15N SQ CPMG |
| 9 | 1 | 5 | 15N SQ CPMG |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | 1 | 278 |
| 2 | 6.5 | 1 | 283 |
Conformers
| Conformers Calculated Total Number | 1100 |
| Conformers Submitted Total Number | 10 |
