6N7O
Crystal structure of GIL01 gp7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08B1-1 |
Synchrotron site | CLSI |
Beamline | 08B1-1 |
Temperature [K] | 85 |
Detector technology | CCD |
Collection date | 2016-07-25 |
Detector | RAYONIX MX300HE |
Wavelength(s) | .9801 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.690, 44.700, 46.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.158 - 1.700 |
R-factor | 0.1951 |
Rwork | 0.193 |
R-free | 0.22970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.678 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 32.158 | 32.158 | 1.510 |
High resolution limit [Å] | 1.470 | 6.570 | 1.470 |
Rmerge | 0.221 | 0.067 | 4.145 |
Rmeas | 0.237 | 0.073 | 4.580 |
Total number of observations | 108259 | ||
Number of reflections | 9511 | 200 | 956 |
<I/σ(I)> | 7.24 | 21.64 | 0.44 |
Completeness [%] | 99.1 | 100 | 91.4 |
Redundancy | 7.497 | 6.175 | 5.613 |
CC(1/2) | 0.995 | 0.997 | 0.154 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 295.15 | 0.2 M sodium iodide, 0.1 M Bis Tris propane, pH 8.5, 20% (w/v) PEG 3.35k |