6N2U
IL-8 Structure from Bacterial Expression Source
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-31 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 39.701, 39.701, 89.971 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.120 - 1.254 |
R-factor | 0.1905 |
Rwork | 0.187 |
R-free | 0.22330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5d14 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.990 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.120 | 1.299 |
High resolution limit [Å] | 1.254 | 1.254 |
Rmerge | 0.026 | 0.322 |
Rmeas | 0.037 | 0.322 |
Rpim | 0.026 | 0.752 |
Number of reflections | 13693 | 122 |
<I/σ(I)> | 15.99 | |
Completeness [%] | 58.8 | 5.34 |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.752 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2.4 M Ammonium Phosphate dibasic, 0.1 M Tris HCl pH 8.5 |