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6N2N

Crystal structure of 2-oxoglutarate:ferredoxin oxidoreductase from Magnetococcus marinus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]100
Detector technologyPIXEL
Collection date2015-08-23
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.97920
Spacegroup nameP 21 21 21
Unit cell lengths86.282, 123.161, 162.487
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution98.152 - 1.937
R-factor0.1698
Rwork0.168
R-free0.20490
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4wbx 5c4i 3g2e
RMSD bond length0.005
RMSD bond angle0.710
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX ((1.12_2829: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]100.0002.010
High resolution limit [Å]1.9371.937
Number of reflections12566311651
<I/σ(I)>7.7
Completeness [%]97.6
Redundancy4
CC(1/2)0.735
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP30014% (w/v) PEG 8000, 0.21-0.28 M (NH4)2SO4, and 0.10 M MES pH 6.5

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