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6MZN

Zebrafish betaglycan orphan domain structure from tetragonal crystal form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]100
Detector technologyCCD
Collection date2017-08-14
DetectorRAYONIX MX300-HS
Wavelength(s)0.9795
Spacegroup nameP 41
Unit cell lengths62.940, 62.940, 114.250
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution27.330 - 2.380
R-factor0.202
Rwork0.198
R-free0.22900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6mzp
RMSD bond length0.010
RMSD bond angle1.270
Data reduction softwareMOSFLM (7.2.2)
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareBUSTER (2.10.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]35.1102.470
High resolution limit [Å]2.3802.380
Rmerge0.0801.784
Rmeas0.0932.104
Rpim0.0460.786
Number of reflections177501873
<I/σ(I)>10.61.1
Completeness [%]99.499.8
Redundancy7.56.8
CC(1/2)0.9980.520
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2988% v/v PEG 5K mono methyl ether, 4% w/v PEG 20K, 0.1M MES pH 6.5

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