6MYI
Pleurotus ostreatus OstreolysinA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.430, 100.335, 59.018 |
Unit cell angles | 90.00, 106.43, 90.00 |
Refinement procedure
Resolution | 33.305 - 1.150 |
R-factor | 0.1419 |
Rwork | 0.142 |
R-free | 0.16060 |
Structure solution method | MIR |
RMSD bond length | 0.018 |
RMSD bond angle | 1.154 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.120 |
High resolution limit [Å] | 1.100 | 2.990 | 1.100 |
Rmerge | 0.046 | 0.031 | 0.915 |
Rmeas | 0.050 | 0.034 | 1.025 |
Rpim | 0.019 | 0.013 | 0.449 |
Number of reflections | 205258 | 10552 | 9347 |
<I/σ(I)> | 7.2 | ||
Completeness [%] | 97.8 | 99 | 89.6 |
Redundancy | 6.2 | 6.8 | 4.4 |
CC(1/2) | 0.999 | 0.631 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.1 M ammonium chloride, 0.05 M tris hydrochloride, 0.15 M sodium chloride, 19% (w/v) PEG3350, 30% (w/v) ethylene glycol |