6MWH
LasR LBD:BB0020 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2017-11-15 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 42.728, 62.067, 50.601 |
| Unit cell angles | 90.00, 91.84, 90.00 |
Refinement procedure
| Resolution | 29.000 - 2.200 |
| R-factor | 0.2044 |
| Rwork | 0.197 |
| R-free | 0.27470 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.271 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.200 | 2.270 |
| High resolution limit [Å] | 2.200 | 2.190 |
| Number of reflections | 12675 | |
| <I/σ(I)> | 16.5 | |
| Completeness [%] | 92.7 | |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 200 mM magnesium nitrate, 20% PEG3350 |
