6MTM
Crystal Structure of EM2 TCR in complex with HLA-B*37:01-NP338
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.806, 97.915, 189.594 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.400 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rpim | 0.134 | 0.391 |
Number of reflections | 18278 | 2614 |
<I/σ(I)> | 6.3 | |
Completeness [%] | 100.0 | |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 19% PEG 3350, 0.2 ammonium tartrate |