6MQU
PL5, synthetic transmembrane domain variant of human phospholamban
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-21 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.1158 |
Spacegroup name | I 41 |
Unit cell lengths | 124.230, 124.230, 51.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 87.840 - 3.170 |
R-factor | 0.229 |
Rwork | 0.228 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.122 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.840 | 3.390 |
High resolution limit [Å] | 3.170 | 3.170 |
Rmerge | 0.171 | 0.540 |
Rpim | 0.314 | |
Number of reflections | 6819 | 1212 |
<I/σ(I)> | 6.2 | 2.7 |
Completeness [%] | 99.0 | 98.2 |
Redundancy | 3.9 | 3.9 |
CC(1/2) | 0.802 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 12 MM C8E4, 20MM MGCL HEXAHYDRATE, 25MM NACL, 50 MM HEPES, 16% PEG400, VAPOR DIFFUSION, TEMPERATURE 298K |