6MPL
Racemic M2-TM I39A crystallized from racemic detergent
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-26 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97856 |
Spacegroup name | P -1 |
Unit cell lengths | 17.120, 18.840, 37.020 |
Unit cell angles | 94.27, 90.02, 109.51 |
Refinement procedure
Resolution | 17.701 - 1.550 |
R-factor | 0.25 |
Rwork | 0.249 |
R-free | 0.26140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rwc |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.701 | 1.605 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmeas | 0.052 | 0.155 |
Rpim | 0.028 | 0.084 |
Number of reflections | 6048 | 577 |
<I/σ(I)> | 12.36 | 5.19 |
Completeness [%] | 95.5 | 93.97 |
Redundancy | 3.4 | 3.5 |
CC(1/2) | 0.998 | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.1 M N-(2-Acetamido)iminodiacetic acid 20% v/v (+/-)-2-Methyl-2,4-pentanediol |