6ML4
BTB24 Zinc Fingers 4-8 with 19+1mer DNA Oligonucleotide (Sequence 3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-003 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-24 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.277, 68.807, 48.434 |
Unit cell angles | 90.00, 92.40, 90.00 |
Refinement procedure
Resolution | 28.039 - 1.482 |
R-factor | 0.1917 |
Rwork | 0.191 |
R-free | 0.21130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ml3 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.532 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.040 | 1.540 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.040 | |
Rpim | 0.019 | 0.530 |
Number of reflections | 40443 | 570 |
<I/σ(I)> | 16.7 | 1.5 |
Completeness [%] | 80.4 | 11.3 |
Redundancy | 4.2 | 1.1 |
CC(1/2) | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 292 | 25% PEG3350, 0.1 M HEPES, pH 7.5, 0.2 M ammonium acetate |