6M8M
PA14 sugar-binding domain from RTX adhesin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 108 |
Detector technology | CCD |
Collection date | 2015-09-19 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.979 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 32.575, 61.309, 79.519 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.550 - 1.200 |
R-factor | 0.141 |
Rwork | 0.140 |
R-free | 0.15850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5j6y |
RMSD bond length | 0.006 |
RMSD bond angle | 1.002 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3120) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.550 | 1.241 |
High resolution limit [Å] | 1.198 | 1.198 |
Number of reflections | 50698 | |
<I/σ(I)> | 27.6 | |
Completeness [%] | 99.6 | |
Redundancy | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 298 | Potassium thiocyanate, Bis Tris Propane (pH 7.5), PEG 3350, Glucose |