6M5F
Crystal structure of HinK, a LysR family transcriptional regulator from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97935 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.534, 152.493, 72.646 |
Unit cell angles | 90.00, 91.80, 90.00 |
Refinement procedure
Resolution | 43.738 - 2.750 |
R-factor | 0.199 |
Rwork | 0.196 |
R-free | 0.25690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fzv |
RMSD bond length | 0.005 |
RMSD bond angle | 0.894 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.800 |
High resolution limit [Å] | 2.750 | 7.460 | 2.750 |
Rmerge | 0.090 | 0.047 | 0.609 |
Rmeas | 0.104 | 0.054 | 0.705 |
Rpim | 0.050 | 0.026 | 0.347 |
Total number of observations | 116999 | ||
Number of reflections | 29609 | 1527 | 1517 |
<I/σ(I)> | 9.8 | ||
Completeness [%] | 98.2 | 98.9 | 98.9 |
Redundancy | 4 | 3.9 | 3.9 |
CC(1/2) | 0.996 | 0.705 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M Ammonium citrate dibasic, 20% w/v Polyethylene glycol 3350 |