6M4R
Structure of Human Serum Albumin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 |
Unit cell lengths | 55.664, 59.099, 86.812 |
Unit cell angles | 90.10, 90.04, 103.60 |
Refinement procedure
Resolution | 19.760 - 2.490 |
R-factor | 0.2342 |
Rwork | 0.232 |
R-free | 0.27360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ao6 |
Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.760 | 2.590 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.073 | 0.686 |
Number of reflections | 36927 | 4168 |
<I/σ(I)> | 8.3 | |
Completeness [%] | 98.0 | |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG |