6M3V
355 bp di-nucleosome harboring cohesive DNA termini
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 98 |
Detector technology | PIXEL |
Collection date | 2019-08-24 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 88.987, 228.970, 118.839 |
Unit cell angles | 90.00, 92.68, 90.00 |
Refinement procedure
Resolution | 49.330 - 4.600 |
R-factor | 0.2061 |
Rwork | 0.205 |
R-free | 0.26050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ut9 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.282 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.330 | 4.920 |
High resolution limit [Å] | 4.600 | 4.600 |
Rmerge | 0.129 | 1.800 |
Rpim | 0.054 | 0.818 |
Number of reflections | 26415 | 4782 |
<I/σ(I)> | 6.6 | 1.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.9 | 6.6 |
CC(1/2) | 0.995 | 0.481 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.5 | 291 | Calcium chloride, Potassium chloride, Potassium Cacodylate, Poly glutamic acid |