6M3H
Crystal structure of mouse HPF1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-12-07 |
Detector | Nonius Kappa CCD |
Wavelength(s) | 0.97849 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.031, 79.895, 106.674 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.360 - 1.710 |
R-factor | 0.1838 |
Rwork | 0.182 |
R-free | 0.21750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6m3g |
RMSD bond length | 0.006 |
RMSD bond angle | 0.943 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.770 |
High resolution limit [Å] | 1.710 | 1.710 |
Rpim | 0.023 | 0.351 |
Number of reflections | 39364 | 2485 |
<I/σ(I)> | 31.1 | |
Completeness [%] | 99.3 | |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 300 | 0.1M Tris-pH8.3, 0.2 M Potassium citrate tribasic monohydrate, 20% w/v PEG 3350, |