6LUK
Crystal structure of the SAMD1 SAM domain in another crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2020-01-15 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97891 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 66.430, 182.842, 66.971 |
Unit cell angles | 90.00, 93.32, 90.00 |
Refinement procedure
Resolution | 45.710 - 2.054 |
R-factor | 0.1872 |
Rwork | 0.185 |
R-free | 0.22590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | A model solved by Se-Met labelled sample. |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.120 |
High resolution limit [Å] | 2.054 | 2.054 |
Rmerge | 0.099 | 0.520 |
Number of reflections | 98440 | 8178 |
<I/σ(I)> | 12.1 | 1.9 |
Completeness [%] | 99.9 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.1M bis-tris (pH 7.5), 2.1M ammonium sulphate |