6LRU
Marsupenaeus japonicus ferritin mutant (T158H)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 273.15 |
Detector technology | CCD |
Collection date | 2019-05-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.4813 |
Spacegroup name | P 4 3 2 |
Unit cell lengths | 117.349, 117.349, 117.349 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.109 - 2.400 |
R-factor | 0.1358 |
Rwork | 0.131 |
R-free | 0.18340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6a4u |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.490 |
High resolution limit [Å] | 2.398 | 5.170 | 2.400 |
Rmerge | 0.237 | 0.099 | 0.722 |
Rmeas | 0.241 | 0.100 | 0.732 |
Rpim | 0.042 | 0.018 | 0.119 |
Number of reflections | 20515 | 1277 | 1109 |
<I/σ(I)> | 8.2 | ||
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 34.3 | 30.8 | 37.5 |
CC(1/2) | 0.999 | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 2000 mM NaCl, 100 mM imidazole (pH 8.0), 2 mM NiSO4 |