6LOL
The crystal structure of full length IpaH9.8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 106.640, 122.250, 149.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 86.910 - 2.750 |
R-factor | 0.248 |
Rwork | 0.246 |
R-free | 0.28490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5b0t |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.910 | 2.848 |
High resolution limit [Å] | 2.750 | 2.750 |
Rmerge | 0.080 | |
Rmeas | 0.087 | |
Number of reflections | 25746 | 2524 |
<I/σ(I)> | 15.74 | 2.56 |
Completeness [%] | 99.5 | 99.41 |
Redundancy | 6.6 | 7 |
CC(1/2) | 0.994 | 0.862 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 3.0M NaCl, 0.1M Na Citrate, pH 6.5 |