6LLZ
Crystal Structure of Fagopyrum esculentum M UGT708C1 complexed with UDP-glucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-25 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 98.914, 143.757, 69.758 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.006 |
R-factor | 0.1696 |
Rwork | 0.168 |
R-free | 0.20150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2acv |
RMSD bond length | 0.008 |
RMSD bond angle | 1.191 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.059 | 50.000 | 1.970 |
High resolution limit [Å] | 1.940 | 5.260 | 1.940 |
Rmerge | 0.089 | 0.068 | 0.363 |
Rmeas | 0.098 | 0.075 | 0.427 |
Rpim | 0.040 | 0.032 | 0.218 |
Number of reflections | 69452 | 3823 | 239 |
<I/σ(I)> | 9.5 | ||
Completeness [%] | 94.4 | 96.3 | 6.6 |
Redundancy | 6.3 | 5.7 | 2.7 |
CC(1/2) | 0.994 | 0.943 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M ammonium sulfate, 0.1M MES pH 7.0, 26.5%(w/v) polyethylene glycol 5000, 26%(w/v) benzamidine hydrochloride, 5mM UDP-glucose |