6LG0
Crystal structure of SbCGTa in complex with UDP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2019-04-14 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97851 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 97.318, 171.593, 179.169 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.958 - 2.998 |
| R-factor | 0.2436 |
| Rwork | 0.242 |
| R-free | 0.27050 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6lfz |
| Data reduction software | DENZO |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.958 | 3.230 |
| High resolution limit [Å] | 2.998 | 3.000 |
| Rpim | 0.095 | 0.689 |
| Number of reflections | 59473 | 11419 |
| <I/σ(I)> | 7.65 | |
| Completeness [%] | 97.6 | |
| Redundancy | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2M Ammonium citrate tribasic pH7.0 20%(w/v) Polyethylene glycol 3,350 |
