6LG0
Crystal structure of SbCGTa in complex with UDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2019-04-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97851 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 97.318, 171.593, 179.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.958 - 2.998 |
R-factor | 0.2436 |
Rwork | 0.242 |
R-free | 0.27050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6lfz |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.958 | 3.230 |
High resolution limit [Å] | 2.998 | 3.000 |
Rpim | 0.095 | 0.689 |
Number of reflections | 59473 | 11419 |
<I/σ(I)> | 7.65 | |
Completeness [%] | 97.6 | |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2M Ammonium citrate tribasic pH7.0 20%(w/v) Polyethylene glycol 3,350 |