6LEE

Crystal structure of Cypovirus Polyhedra mutant with deletion of Ala67-Ala104

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-06-30
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1
Spacegroup name	I 2 3
Unit cell lengths	103.840, 103.840, 103.840
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.430 - 1.950
R-factor	0.19339
Rwork	0.187
R-free	0.25025
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2oh6
RMSD bond length	0.009
RMSD bond angle	1.635
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	REFMAC (5.8.0238)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.070
High resolution limit [Å]	1.950	1.950
Rmeas	0.808	2.959
Number of reflections	13756	2222
<I/σ(I)>	4.73	1.27
Completeness [%]	100.0
Redundancy	23.4
CC(1/2)	0.967	0.562

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	IN CELL		293	in cell crysrallization