6LCT
Crystal structure of catalytic inactive chloroplast resolvase NtMOC1 in complex with Holliday junction
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 121.054, 89.807, 68.478 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.350 - 2.550 |
R-factor | 0.2211 |
Rwork | 0.220 |
R-free | 0.24490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kvo |
RMSD bond length | 0.003 |
RMSD bond angle | 0.517 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.350 | 2.660 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.030 | 0.727 |
Rmeas | 0.036 | 0.789 |
Rpim | 0.014 | 0.418 |
Number of reflections | 24991 | 2962 |
<I/σ(I)> | 28.2 | 2.6 |
Completeness [%] | 99.9 | |
Redundancy | 6.5 | 6.7 |
CC(1/2) | 0.999 | 0.812 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291.15 | PEG 4000, Sodium acetate trihydrate, 3-Methyl-1,5-Pentane Diol, D-sorbitol |