6LBU
Crystal structure of yeast Stn1 and Ten1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.306, 78.031, 101.151 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.951 - 2.000 |
R-factor | 0.2135 |
Rwork | 0.211 |
R-free | 0.25750 |
Structure solution method | SAD |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.088 | 0.062 | 0.372 |
Rmeas | 0.092 | 0.064 | 0.389 |
Rpim | 0.026 | 0.018 | 0.110 |
Total number of observations | 314501 | ||
Number of reflections | 24869 | 2698 | 2338 |
<I/σ(I)> | 4.6 | ||
Completeness [%] | 99.5 | 100 | 95.7 |
Redundancy | 12.6 | 12.1 | 11.3 |
CC(1/2) | 0.999 | 0.979 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.5 | 277 | 0.2 M potassium chloride, 0.05 M Sodium cacodylate trihydrate, 10% (w/v) PEG4000 |