6LBC
shrimp ferritin-T158R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | I 4 |
Unit cell lengths | 124.783, 124.783, 175.395 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.460 - 1.801 |
R-factor | 0.1952 |
Rwork | 0.195 |
R-free | 0.22540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6a4u |
RMSD bond length | 0.006 |
RMSD bond angle | 0.770 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 3.880 | 1.800 |
Rmerge | 0.148 | 0.070 | 0.927 |
Rmeas | 0.160 | 0.076 | 1.004 |
Rpim | 0.061 | 0.029 | 0.385 |
Total number of observations | 839727 | ||
Number of reflections | 123173 | 12426 | 12249 |
<I/σ(I)> | 3.7 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 6.8 | 6.8 | 6.7 |
CC(1/2) | 0.995 | 0.626 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.5 | 293.15 | 0.1 M Tris pH 8.5, 2.0 M Ammonium sulfate |