6L8P
Crystal structure of RidA from Antarctic bacterium Psychrobacter sp. PAMC 21119
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-24 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.284, 71.141, 108.479 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.227 - 1.601 |
R-factor | 0.1487 |
Rwork | 0.148 |
R-free | 0.16400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3k0t |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.630 |
High resolution limit [Å] | 1.600 | 4.340 | 1.600 |
Rmerge | 0.106 | 0.069 | 0.486 |
Rmeas | 0.115 | 0.075 | 0.523 |
Rpim | 0.044 | 0.029 | 0.193 |
Total number of observations | 479686 | ||
Number of reflections | 69280 | 3727 | 3385 |
<I/σ(I)> | 10.6 | ||
Completeness [%] | 100.0 | 99.8 | 100 |
Redundancy | 6.9 | 6.9 | 7.4 |
CC(1/2) | 0.995 | 0.924 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Bis-Tris Propane/HCl (pH 7), 1.1 M malonic acid, 0.15 M ammonium citrate tribasic, 0.072 M succinic acid, 0.18 M DL-malic acid, 0.24 M sodium acetate, 0.3 M sodium formate, and 0.1 M ammonium tartrate dibasic |